An innovative approach to SFC-MS and Open Bed fraction collection.
- Single quadrupole MS detector
- Collection using up to 4 mass values
- Specially designed miniature cyclones
- Up to 100 ml/min flow rates
- At-tube GLS
- No make-up solvents,
- No fraction dilution
- No fraction collection timing issues
- Automated wash sequences eliminate cross contamination.
Mass-directed collection is based upon up to 4 mass values, entered in the separation method. As many as 242 collection tubes are available in 2 racks for collection with a sample capacity of 72 x 10 ml vials which ensure that the system runs continuously and efficiently through multiple separations. The collection tubes may be filled up to 90% of their volume. A dual collection head system is also available which reduces potential for sample loss.
The systems are based upon the proven SFC-PICLab PREP 100 and SFC-PICLab Hybrid 10-100 systems, the latter unit allowing automated method development at the analytical scale with 9 analytical column and 6 co-solvent selection through PIC Solutionís proprietary software as well as preparative capability. The units can hold up to 6 preparative columns on a software-driven selection valve. The Hybrid system can be programmed to run post-separation analyses on the collected fractions from the collection tubes.
|Flow Rate||100 ml/min|
|Co-solvent Flow Rate||50 ml/min|
|Maximum Pressure||350 bar|
|Co-Solvents||Selected from 6|
|Analytical Columns (Hybrid)||Selected from 9|
|Preparative Columns||Selected from 6|
|Temperature||20 to 60°C|
|Detector||DAD UV (4 simultaneous wavelengths) / MS (4 mass values)|
|Power||110V; 60 Hz; 20 A|
|Dimensions||140 x 75 x 120 cm|